Publication detail

Effects of thermal annealing as polymer processing step on poly(lactic acid)

Miroslav Pastorek, Adriana Kovalcik

Original Title

Effects of thermal annealing as polymer processing step on poly(lactic acid)

Type

journal article in Web of Science

Language

English

Original Abstract

Thermal annealing as an additional polymer processing step or post-treatment processing step enables the structural changes of amorphous parts into crystalline parts. This paper investigates the feasibility of thermal annealing at 100 degrees C up to 90min used as an additional processing step to modify the crystalline structure and the thermo-mechanical stability of poly(lactic acid) (PLA). Moreover, the crystallization ability of PLA has been amended by the addition of 3wt% of wood flour and kaolin. The values of the degree of crystallinity and lamellar thickness determined by wide-angle-X-ray scattering showed that the thermal annealing of PLA samples modified with nucleating agents was an efficient processing step to increase the final crystallinity of PLA. Moreover, altered crystalline structure helped to improve the thermomechanical stability of PLA.

Keywords

Additives; annealing; creep; crystallinity; kaolin; nucleation; poly(lactic acid); processing; stability; thermoforming; wood

Authors

Miroslav Pastorek, Adriana Kovalcik

Released

28. 3. 2018

Publisher

TAYLOR & FRANCIS INC, 530 WALNUT STREET, STE 850, PHILADELPHIA, PA 19106 USA

Location

530 WALNUT STREET, STE 850, PHILADELPHIA, PA 19106 USA

ISBN

1532-2475

Periodical

Materials and Manufacturing Processes

Year of study

33

Number

15

State

United States of America

Pages from

1674

Pages to

1680

Pages count

7

URL

BibTex

@article{BUT150182,
  author="Adriána {Kovalčík}",
  title="Effects of thermal annealing as polymer processing step on poly(lactic acid)",
  journal="Materials and Manufacturing Processes",
  year="2018",
  volume="33",
  number="15",
  pages="1674--1680",
  doi="10.1080/10426914.2018.1453153",
  issn="1532-2475",
  url="https://www.tandfonline.com/doi/full/10.1080/10426914.2018.1453153"
}