Publication result detail
IR-Supported Thermogravimetric Analysis of Water in Hydrogels
ENEV, V.; SEDLÁČEK, P.; ŘIHÁK, M.; KALINA, M.; PEKAŘ, M.
Original Title
IR-Supported Thermogravimetric Analysis of Water in Hydrogels
English Title
IR-Supported Thermogravimetric Analysis of Water in Hydrogels
Type
WoS Article
Original Abstract
Isothermal thermogravimetry in a kinetic mode and time-resolved infrared spectroscopy was used to characterize water and its binding in hydrogels formed by interactions between hyaluronan and micelles of Septonex, an oppositely charged surfactant. Thermogravimetry provided detailed insight into the dehydration kinetics of the gel and thus brought indirect information on the strength of water binding in the hydrogel network. Infrared (IR) spectroscopy complemented the study with a direct analysis of structural changes occurring in the gel during its dehydration. IR spectroscopy thus contributed to understanding the processes which were observed in thermogravimetry, qualitatively, on the molecular level. This study can contribute to a broader application of the combined thermogravimetry–IR approach in the study of hydrogel materials and the development of their applications, especially in bio-related areas where water is among the key players.
English abstract
Isothermal thermogravimetry in a kinetic mode and time-resolved infrared spectroscopy was used to characterize water and its binding in hydrogels formed by interactions between hyaluronan and micelles of Septonex, an oppositely charged surfactant. Thermogravimetry provided detailed insight into the dehydration kinetics of the gel and thus brought indirect information on the strength of water binding in the hydrogel network. Infrared (IR) spectroscopy complemented the study with a direct analysis of structural changes occurring in the gel during its dehydration. IR spectroscopy thus contributed to understanding the processes which were observed in thermogravimetry, qualitatively, on the molecular level. This study can contribute to a broader application of the combined thermogravimetry–IR approach in the study of hydrogel materials and the development of their applications, especially in bio-related areas where water is among the key players.
Keywords
hydration, hydrogel, IR spectroscopy, thermogravimetry, water binding
Key words in English
hydration, hydrogel, IR spectroscopy, thermogravimetry, water binding
Authors
ENEV, V.; SEDLÁČEK, P.; ŘIHÁK, M.; KALINA, M.; PEKAŘ, M.
RIV year
2023
Released
06.06.2022
Publisher
Frontiers
Location
Švýcarská konfederace
ISBN
2296-8016
Periodical
Frontiers in Materials
Volume
9
Number
Červenec
State
Swiss Confederation
Pages from
1
Pages to
8
Pages count
8
URL
BibTex
@article{BUT179331,
author="Vojtěch {Enev} and Petr {Sedláček} and Marek {Řihák} and Michal {Kalina} and Miloslav {Pekař}",
title="IR-Supported Thermogravimetric Analysis of Water in Hydrogels",
journal="Frontiers in Materials",
year="2022",
volume="9",
number="Červenec",
pages="1--8",
doi="10.3389/fmats.2022.931303",
issn="2296-8016",
url="https://www.frontiersin.org/articles/10.3389/fmats.2022.931303/full"
}