Publication result detail
Synthesis and processing of InVO4
BARTONÍČKOVÁ, E.; CIHLÁŘ, J.
Original Title
Synthesis and processing of InVO4
English Title
Synthesis and processing of InVO4
Type
Peer-reviewed article not indexed in WoS or Scopus
Original Abstract
Indium vanadates for severe applications as photocatalysts, anodes for Li rechargeable batteries or electrochromic devices were prepared via conventional and non-conventional preparation methods. The conventional high temperature solid state reaction was performed at 800 C for 25 hours and the non-conventional microwave-assisted synthesis was performed at 220 C for different reaction times under hydrothermal conditions. The as-prepared powders were characterized in terms of phase composition by X-Ray diffraction analysis (XRD) and infrared spectroscopy (IR) and of powder morphology by scanning electron microscopy (SEM) and BET method. Nanosized indium vanadate powders were successfully synthesized by non-conventional microwave-assisted hydrothermal method. The dense ceramic bodies suitable for electrical conductivity measurements with 96% t.d. were obtained by sintering of powders prepared by high-temperature solid state reaction at 1100 C for 4 h with admission of oleic acid as a binder additive
English abstract
Indium vanadates for severe applications as photocatalysts, anodes for Li rechargeable batteries or electrochromic devices were prepared via conventional and non-conventional preparation methods. The conventional high temperature solid state reaction was performed at 800 C for 25 hours and the non-conventional microwave-assisted synthesis was performed at 220 C for different reaction times under hydrothermal conditions. The as-prepared powders were characterized in terms of phase composition by X-Ray diffraction analysis (XRD) and infrared spectroscopy (IR) and of powder morphology by scanning electron microscopy (SEM) and BET method. Nanosized indium vanadate powders were successfully synthesized by non-conventional microwave-assisted hydrothermal method. The dense ceramic bodies suitable for electrical conductivity measurements with 96% t.d. were obtained by sintering of powders prepared by high-temperature solid state reaction at 1100 C for 4 h with admission of oleic acid as a binder additive
Keywords
Indium vanadate; microwave-assisted hydrothermal synthesis
Key words in English
Indium vanadate; microwave-assisted hydrothermal synthesis
Authors
BARTONÍČKOVÁ, E.; CIHLÁŘ, J.
RIV year
2011
Released
08.01.2010
Publisher
WORLD SCIENTIFIC PUBL CO PTE LTD
Location
5 TOH TUCK LINK, SINGAPORE 596224, SINGAPORE
ISBN
0217-9792
Periodical
INTERNATIONAL JOURNAL OF MODERN PHYSICS B
Volume
24
Number
6-7
State
Republic of Singapore
Pages from
770
Pages to
779
Pages count
10
BibTex
@article{BUT49500,
author="Eva {Bartoníčková} and Jaroslav {Cihlář}",
title="Synthesis and processing of InVO4",
journal="INTERNATIONAL JOURNAL OF MODERN PHYSICS B",
year="2010",
volume="24",
number="6-7",
pages="770--779",
issn="0217-9792"
}