Publication result detail

Wastewater preconcentration method for the determination of legislation limits of cadmium, arsenic, zinc, copper, nickel, chromium and lead employing portable ED -XRF

Sýkora, Komendová

Original Title

Wastewater preconcentration method for the determination of legislation limits of cadmium, arsenic, zinc, copper, nickel, chromium and lead employing portable ED -XRF

English Title

Wastewater preconcentration method for the determination of legislation limits of cadmium, arsenic, zinc, copper, nickel, chromium and lead employing portable ED -XRF

Type

Abstract

Original Abstract

The chemical laboratories of the Fire Rescue Service of the Czech Republic (hereinafter referred to as CHL FRS) encounter the issue of determining hazardous metals in wastewater or surface water several times a year. The determination of hazardous metals such as arsenic, copper, lead, zinc, chromium, nickel or cadmium can be problematic, since not all CHL FRS have available instrumentation infrastructure such as ICP­OES or ICP‑MS, for determination of trace amounts of heavy metals in samples. However, all CHL FRS have a mobile energy­dispersive X­ray fluorescence analyzer Delta X (hereinafter ED­XRF). The detection limits of ED­XRF for abovementioned elements are at a concentration level of 10 mg/l. The limits for selected elements in the surface water and wastewater are specified in Government Regulation No. 401/2015 Coll. from tenths to several mg /l If CHL FRS are to achieve these values by ED­XRF, it is necessary to use an effective preconcentration technique.

English abstract

The chemical laboratories of the Fire Rescue Service of the Czech Republic (hereinafter referred to as CHL FRS) encounter the issue of determining hazardous metals in wastewater or surface water several times a year. The determination of hazardous metals such as arsenic, copper, lead, zinc, chromium, nickel or cadmium can be problematic, since not all CHL FRS have available instrumentation infrastructure such as ICP­OES or ICP‑MS, for determination of trace amounts of heavy metals in samples. However, all CHL FRS have a mobile energy­dispersive X­ray fluorescence analyzer Delta X (hereinafter ED­XRF). The detection limits of ED­XRF for abovementioned elements are at a concentration level of 10 mg/l. The limits for selected elements in the surface water and wastewater are specified in Government Regulation No. 401/2015 Coll. from tenths to several mg /l If CHL FRS are to achieve these values by ED­XRF, it is necessary to use an effective preconcentration technique.

Keywords

Cd, As, Zn, Cu, Ni, Cr, Pb, ED­‑XRF, preconcentration, wastewater

Key words in English

Cd, As, Zn, Cu, Ni, Cr, Pb, ED­‑XRF, preconcentration, wastewater

Authors

Sýkora, Komendová

RIV year

2022

Released

25.11.2021

Publisher

Vysoké učení technické v Brně, Fakulta chemická,

Location

Brno

ISBN

978-80-214-6002-7

Book

Sborník abstraktu

Pages from

61

Pages to

62

Pages count

106

URL

https://www.fch.vut.cz/vav/konference/sok/vystupy/sbornik-konference-2021-abstrakty-a5-pdf-p213391

Full text in the Digital Library

http://hdl.handle.net/

BibTex

@misc{BUT175465,
  author="Jiří {Sýkora} and Renata {Komendová}",
  title="Wastewater preconcentration method for the determination of legislation limits of cadmium, arsenic, zinc, copper, nickel, chromium and lead employing portable ED -XRF",
  booktitle="Sborník abstraktu",
  year="2021",
  edition="první",
  pages="61--62",
  publisher="Vysoké učení technické v Brně, Fakulta chemická,",
  address="Brno",
  isbn="978-80-214-6002-7",
  url="https://www.fch.vut.cz/vav/konference/sok/vystupy/sbornik-konference-2021-abstrakty-a5-pdf-p213391",
  note="Abstract"
}