Course detail
Methods of structure analysis
FCH-MCT_MSAAcad. year: 2015/2016
Overwiev of structural organic analysis. Ultra-violet and infra-red spectroscopy. Nuclear magnetic resonance of 1H and 13C nucleus. Mass spectrometry.
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Learning outcomes of the course unit
1. Students will be thoroughly familiar with the physical principles of structural analysis methods and with their information abilityin the structural analysis of organic compounds
2. Students will master the procedures of UV-VIS, IR, MS and NMR spectra interpretation for the structural analysis of organic compounds
3. Students will be able to complete the partial information obtained from UV-VIS, IR, MS and NMR spectra in order to identify unknown compounds.
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
Course curriculum
2. Interpretation of IR spectra.
3. Intepretation of 1D 1H NMR spectra.
4. Interpretation of 1D 13C NMR spectra.
5.-6. 2D NMR and interpretation of 2D NMR spectra..
7. NMR spectra of sselected groups of organic compounds.
8. Interpretation of MS spectra using hard ionization technique.
9. Interpretation of MS spectra using soft ionization technique.
10. Interpretation of high resolution mass spectra.
11.-13. Practical examples of structural analysis based on the interpretation of the spectrum files.
Work placements
Aims
- Learning of the physical basics of structural-analytical methods (UV-VIS spectrophotometry, infrared spectrometry, mass spectrometry, nuclear magnetic resonance)
- Mastering of interpretation of UV-VIS, IR, MS and NMR spectra at the lower intermediate level
- Adopting of combination of information obtained from individual spectra in order to determine the structure of organic compounds.
Specification of controlled education, way of implementation and compensation for absences
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Recommended reading
Classification of course in study plans
- Programme NPCP_CHTOZP Master's
branch NPCO_CHTOZP , 1 year of study, summer semester, compulsory-optional
- Programme NKCP_CHTOZP Master's
branch NKCO_CHTOZP , 1 year of study, summer semester, compulsory-optional
- Programme CKCP_CZV lifelong learning
branch CKCO_CZV , 1 year of study, summer semester, compulsory-optional