Course detail
Methods of Instrumental Analysis
FCH-MC_MIAAcad. year: 2022/2023
Instrumental techniques for characterization of properties of colloids (particles size and charge, interactions, thermodynamic and transport properties) and surface (wetting, contact angle, atomic force microscopy), methods for analysis of colloidal and special materials (thermic, viscoelastic, electric and electro-optical properties, microscopy).
Language of instruction
Number of ECTS credits
Mode of study
Guarantor
Learning outcomes of the course unit
Prerequisites
Co-requisites
Planned learning activities and teaching methods
Assesment methods and criteria linked to learning outcomes
Course curriculum
1. Size distribution of particles and macromolecules (light scattering, SEC)
2. Charge (zeta potential) and wetting of surface, contact angle
3. Atomic force microscopy (AFM)
4. Microcalorimetry (DSC, ITC, IC)
5. Transport properties (sorption and diffusion techniques
Materials analysis
6. Thermochemical analysis (DSC, TG)
7. Rheology and viscometry
8. Electric and electro-optical properties
9. Microscopy (optical and electron)
10.-13. Practical excursions, measurement and data processing
Work placements
Aims
Specification of controlled education, way of implementation and compensation for absences
Recommended optional programme components
Prerequisites and corequisites
Basic literature
Sommer, L.: Teoretické základy analytické chemie I, II, III, VUTIUM, 1995, 1998, 2000. (CS)
Klouda, P.: Moderní analytické metody, Ostrava: Nakladatelství Pavel Klouda, 1996.
Bartovská, L.; Šišková, M.: Fyzikální chemie povrchů a koloidních soustav, Praha: VŠCHT, 2005. (CS)
Recommended reading
Podzimek, Š.: Light Scattering, Size Exclusion Chromatography and AF4, Wiley, 2015. (EN)
Mezger, T.G.: Applied Rheology, Anton Paar, 2014. (EN)
eLearning
Classification of course in study plans
- Programme NPCP_CHCHTE Master's, 1. year of study, winter semester, compulsory
- Programme NKCP_CHCHTE Master's, 1. year of study, winter semester, compulsory
Type of course unit
Lecture
Teacher / Lecturer
Guided consultation in combined form of studies
Teacher / Lecturer
eLearning