Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BCA_ANC2_PAcad. year: 2014/2015

Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, ionex chromatography, electrogravimetry.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

doc. Mgr. Renata Komendová, Ph.D.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Learning outcomes of the course unit

After students finished this course, their competence inceased as follows:

1. They were practical introduced with selected analytical methods.
2. Students be able to practical aplly selected technique of determinations.
3. They practise precise work in analytical laboratory, preparation of standard solutions, good laboratory practise with samples.
4. Students will be able to use of necessary calculations and they will be used evaluation of analytical data from using analysis.

Prerequisites

Laboratory course of analytical chemistry I.

Co-requisites

Not applicable.

Planned learning activities and teaching methods

The course uses teaching methods in form of Laboratory exercise - 5 teaching hours per week. The e-learning system (LMS Moodle) is available to teachers and students.

Assesment methods and criteria linked to learning outcomes

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test (15-20 questions)
Final classification is based on average classification of individual tasks.
Classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F

Course curriculum

Introduction, work safety, analytical laboratory techniques
Redox and potentiometric titrations
Potentiometric titrations (precipitation titrations)
Automatic acid-base titrations
Titrations in nonaqueous solvents
Spectrophotometry
Spectrophotometry in mixtures
Extraction spectrophotometry
Fluorimetry
Emission flame spectrometry
Chromatographic methods (TLC, IEC)
Analysis of copper-based alloys

Work placements

Not applicable.

Aims

The aim of practical classes of analytical chemistry II is to learn students the base and using of selected analytical instrumental methods, such as potentiometry, automatic titration, spectrophotometry, fluorimetry, emission flame spectrometry, TLC, chromatography and electrogravimetry.

Specification of controlled education, way of implementation and compensation for absences

Written entrance tests at the beginning of all exercises checking the students readiness for practical work.
Elaboration of the protocols on a given exercises.
Credit test at the course end.

Recommended optional programme components

Not applicable.

Prerequisites and corequisites

Not applicable.

Basic literature

Komendová R., Praktikum z analytické chemie II, BCA_ANC2_P, https://www.vutbr.cz/elearning/ (CS)
Šimek Z., Komendová R., Mašek I., Voznica P. : Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)

Type of course unit

Laboratory exercise

52 hod., compulsory

Teacher / Lecturer

doc. MVDr. Helena Zlámalová Gargošová, Ph.D.
Jitka Pochopová
Ing. Josef Kotlík, CSc.
Ing. František Mikšík, Ph.D.
doc. Mgr. Renata Komendová, Ph.D.
Ing. Pavlína Modlitbová, Ph.D.
Ing. Veronika Řezáčová, Ph.D.
RNDr. Helena Půčková
Ing. Ludmila Damborská
Ing. Ludmila Mravcová, Ph.D.