Course detail
Methods of Instrumental Analysis
FCH-MA_MIAAcad. year: 2023/2024
Instrumental techniques for characterization of properties of colloids (particles size and charge, interactions, thermodynamic and transport properties) and surface (wetting, contact angle, atomic force microscopy), methods for analysis of colloidal and special materials (thermic, viscoelastic, electric and electro-optical properties, microscopy).
Language of instruction
English
Number of ECTS credits
4
Mode of study
Not applicable.
Guarantor
Offered to foreign students
The home faculty only
Entry knowledge
physical chemistry, analytical chemistry
Rules for evaluation and completion of the course
Written and oral exam.
Attendance to lectures is not required but is recommended.
Attendance to lectures is not required but is recommended.
Aims
The main aim of the course is to describe the principles of selected techniques of instrumental analysis, methods used for characterisation of colloidal systems and materials generally used in modern chemistry, chemical technology and in surface analysis. Describe the ways how to select appropriate instrumental technique, settings the measurement parameters and data processing.
Students attending the course will be able to describe the basic principles of selected methods of structural analysis and methods for characterisation of colloidal systems and materials used in modern chemistry and chemical technology and for surface analysis. Student will be able to select appropriate method for given analysis, its basic settings and make data processing.
Students attending the course will be able to describe the basic principles of selected methods of structural analysis and methods for characterisation of colloidal systems and materials used in modern chemistry and chemical technology and for surface analysis. Student will be able to select appropriate method for given analysis, its basic settings and make data processing.
Study aids
Not applicable.
Prerequisites and corequisites
Not applicable.
Basic literature
Skoog, D. A, Holler, J.: Principles of instrumental analysis, Cengage Learning, 2017.
Sommer, L.: Teoretické základy analytické chemie I, II, III, VUTIUM, 1995, 1998, 2000.
Klouda, P.: Moderní analytické metody, Ostrava: Nakladatelství Pavel Klouda, 1996.
Bartovská, L.; Šišková, M.: Fyzikální chemie povrchů a koloidních soustav, Praha: VŠCHT, 2005.
Sommer, L.: Teoretické základy analytické chemie I, II, III, VUTIUM, 1995, 1998, 2000.
Klouda, P.: Moderní analytické metody, Ostrava: Nakladatelství Pavel Klouda, 1996.
Bartovská, L.; Šišková, M.: Fyzikální chemie povrchů a koloidních soustav, Praha: VŠCHT, 2005.
Recommended reading
Harris, D.C.: Exploring Chemican Analysis, W. H. Freeman, 2012.
Podzimek, Š.: Light Scattering, Size Exclusion Chromatography and AF4, Wiley, 2015.
Mezger, T.G.: Applied Rheology, Anton Paar, 2014.
Podzimek, Š.: Light Scattering, Size Exclusion Chromatography and AF4, Wiley, 2015.
Mezger, T.G.: Applied Rheology, Anton Paar, 2014.
Classification of course in study plans
- Programme NPAP_ENVI Master's, 1. year of study, winter semester, compulsory
- Programme NKCP_CHCHTE Master's, 1. year of study, winter semester, compulsory
- Programme NPCP_CHCHTE Master's, 1. year of study, winter semester, compulsory
Type of course unit
Lecture
26 hours, optionally
Teacher / Lecturer
Syllabus
Characterization of colloidal systems and surfaces
1. Size distribution of particles and macromolecules (light scattering, SEC)
2. Charge (zeta potential) and wetting of surface, contact angle
3. Atomic force microscopy (AFM)
4. Chemical and struktural analysis of dispersions
5. Transport properties (sorption and diffusion techniques
Materials analysis
6. Thermochemical analysis and microcalorimetry (DSC, TG, ITC)
7. Rheology and viscometry
8. Technology of thin layers preparation
9. Electric and electro-optical properties
10. Microscopy (optical and electron)
1. Size distribution of particles and macromolecules (light scattering, SEC)
2. Charge (zeta potential) and wetting of surface, contact angle
3. Atomic force microscopy (AFM)
4. Chemical and struktural analysis of dispersions
5. Transport properties (sorption and diffusion techniques
Materials analysis
6. Thermochemical analysis and microcalorimetry (DSC, TG, ITC)
7. Rheology and viscometry
8. Technology of thin layers preparation
9. Electric and electro-optical properties
10. Microscopy (optical and electron)