Course detail

Laboratory Classes in Physical Chemistry II

FCH-BC_FCH2_PAcad. year: 2023/2024

1. General information, laboratory rules and safety.
In following 11 weeks, students have to get through these laboratory problems:
2. Activation energy of acetone iodization.
3. Decomposition of acetic anhydride.
4. Kinetics of catalytic reaction.
5. Photometric study of kinetics of chemical reactions.
6. Preparation and characterization of emulsions.
7. Rheology of gel systems.
8. Sedimentation analysis of suspensions.
9. Coagulation of lyophobic colloids.
10. Adsorption from solution on solid surface.
11. Influence of adsorption on surface tension of liquids.
12. Principles of electrophoresis.
13. Test + Credits.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

prof. Ing. Martina Klučáková, Ph.D.

Department

Institute of Physical and Applied Chemistry (ÚFSCH)

Entry knowledge

basic knowledge of general and inorganic chemistry, chemical calculations

Rules for evaluation and completion of the course

conditions of graded course-unit credit:
100% active participation in laboratory exercises
get through all laboratory tasks
laboratory reports of all task
classification of all laboratory reports (min. degree E)
classification of laboratory log (min. degree E)
written exam (min. degree E)
total classification min. degree E
classification of all laboratory reports
laboratory log
credit test
...In order to be awarded the course-unit credit students must prove 100% active participation in laboratory exercises and elaborate a paper on the presented themes. The exam is written and oral. In the written part a student compiles two main themes which were presented during the lectures and solves three examples. The oral part of the exam will contain discussion of tasks and possible supplementary questions.
Attendance and activity at the seminars are required. One excused absence can be compensated for by attending a seminar with another group, or by attending in last week of the term.

Aims

The aim of the subject is to acquaint students with practical problems of kinetics and colloidal chemistry. The students should learn to use their theoretical knowledge of physical chemistry in solving of practical problems in laboratory.
The students should obtain practical skills in basic experimental methods of chemical kinetics and colloidal chemistry and in experimental data assessment.

Study aids

Not applicable.

Prerequisites and corequisites

compulsory prerequisite
- Laboratory Classes in Inorganic Chemistry I

Basic literature

Pekař M., Klučáková M., Veselý M., Čeppan M.: Fyzikální chemie a fotochemie. Praktikum. FCH VUT v Brně, Brno, 2007. (CS)

Type of course unit

Laboratory exercise

39 hours, compulsory

Teacher / Lecturer

doc. Ing. Vojtěch Enev, Ph.D.
Ing. Adam Jugl, Ph.D.
prof. Ing. Martina Klučáková, Ph.D.
Ing. Ivana Málková
doc. Ing. Filip Mravec, Ph.D.
Ing. Jiří Smilek, Ph.D.
Ing. Tereza Venerová, Ph.D.
prof. Ing. Martina Klučáková, Ph.D.

Syllabus

1. General information, laboratory rules and safety.
In following 12 weeks, students have to get through these laboratory problems:
2. Activation energy of acetone iodization.
3. Decomposition of acetic anhydride.
4. Kinetics of catalytic reaction.
5. Photometric study of kinetics of chemical reactions.
6. Preparation and characterization of emulsions.
7. Rheology of gel systems.
8. Sedimentation analysis of suspensions.
9. Coagulation of lyophobic colloids.
10. Adsorption from solution on solid surface.
11. Influence of adsorption on surface tension of liquids.
12. Principles of electrophoresis.
13. Test + Credits.

eLearning

eLearning: currently opened course