Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BC_ANC2_PAcad. year: 2023/2024

Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, chromatography, voltammetry, electrogravimetry.

Language of instruction

Czech

Number of ECTS credits

Mode of study

Not applicable.

Guarantor

doc. Mgr. Renata Komendová, Ph.D.

Department

Institute of Chemistry and Technology of Environmental Protection (ÚCHTOŽP)

Entry knowledge

Laboratory course of analytical chemistry I. Practical knowledge of basic laboratory skills: weighing, pipetting, preparation of measuring solutions, titration.
Knowledge of basic calculations used in analytical chemistry, evaluation by the calibration curve method.

Rules for evaluation and completion of the course

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test
Final classification is based on average classification of individual tasks.
Analytical results evaluation:
error to
1.5% A
3% B
5% C
7% D
9% E
error over 9% F
Overall classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F
Input e-learning tests to check students' readiness.
Work in analytical laboratory.
Evaluation of analytical results.
Elaboration of the protocols.
Credit test at the end of the course.

Aims

The aim of practical classes of analytical chemistry II is to learn students the base and using of selected analytical instrumental methods, such as potentiometry, automatic titration, spectrophotometry, fluorimetry, emission flame spectrometry, TLC, chromatography, voltammetry and electrogravimetry.
After students finished this course, their competence inceased as follows:

1. They were practical introduced with selected analytical methods.
2. Students be able to practical aplly selected technique of determinations.
3. They practise precise work in analytical laboratory, preparation of standard solutions, good laboratory practise with samples.
4. Students will be able to use of necessary calculations and they will be used evaluation of analytical data from using analysis.

Study aids

Not applicable.

Prerequisites and corequisites

compulsory prerequisite
- Laboratory Classes in Inorganic Chemistry I

Basic literature

Šimek Z., Komendová R., Mašek I., Voznica P. : Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)

Type of course unit

Laboratory exercise

52 hours, compulsory

Teacher / Lecturer

Ing. Anna Amrichová
Ing. Kristýna Bilavčíková
Ing. Hana Hlaváčková
Pavla Kleinová
doc. Mgr. Renata Komendová, Ph.D.
Ing. Petra Kryštofová
Ing. Martina Machalová
Ing. Ludmila Mravcová, Ph.D.
Mgr. Marie Novotná, Ph.D.
Ing. Veronika Řezáčová, Ph.D.
doc. Mgr. Renata Komendová, Ph.D.

Syllabus

1. Introduction to practice, safety of work, methodology of work in analytical laboratory
2. Precipitation titration (Argentometry)
3. Automatic titration (alkalimetry)
4. Titration in a non-aqueous medium
5. Spectrophotometry
6. Multi-component analysis
7. Fluorimetry
8. Emission flame spectrometry
9. Voltammetry and electrogravimetry
10. Extraction spectrophotometry
11. Liquid Chromatography
12. Thin-layer chromatography

eLearning

eLearning: currently opened course