Course detail

Laboratory Classes in Analytical Chemistry II

FCH-BC_ANC2_PAcad. year: 2024/2025

Practical training at selected basic instrumental analytical methods: potentiometry, automatic titrations, spectrophotometry, fluorimetry, emission flame photometry, thin-layer chromatography, chromatography, voltammetry, electrogravimetry.

Language of instruction

Czech

Number of ECTS credits

3

Mode of study

Not applicable.

Entry knowledge

Laboratory course of analytical chemistry I. Practical knowledge of basic laboratory skills: weighing, pipetting, preparation of measuring solutions, titration.
Knowledge of basic calculations used in analytical chemistry, evaluation by the calibration curve method.

Rules for evaluation and completion of the course

Graded course-unit credit
Requirements:
- all laboratory tasks completed, results and reports in good quality
- course test
Final classification is based on average classification of individual tasks.
Analytical results evaluation:
error to
1.5% A
3% B
5% C
7% D
9% E
error over 9% F
Overall classification:
100-90% A
89-80% B
79-70% C
69-60% D
59-50% E
49-0% F
Input e-learning tests to check students' readiness.
Work in analytical laboratory.
Evaluation of analytical results.
Elaboration of the protocols.
Credit test at the end of the course.

Aims

The aim of practical classes of analytical chemistry II is to learn students the base and using of selected analytical instrumental methods, such as potentiometry, automatic titration, spectrophotometry, fluorimetry, emission flame spectrometry, TLC, chromatography, voltammetry and electrogravimetry.
After students finished this course, their competence inceased as follows:

1. They were practical introduced with selected analytical methods.
2. Students be able to practical aplly selected technique of determinations.
3. They practise precise work in analytical laboratory, preparation of standard solutions, good laboratory practise with samples.
4. Students will be able to use of necessary calculations and they will be used evaluation of analytical data from using analysis.


Study aids

Not applicable.

Prerequisites and corequisites

Basic literature

Šimek Z., Komendová R., Mašek I., Voznica P. : Kvantitativní analýza. FCH VUT v Brně, Brno 2003. (CS)

Recommended reading

Not applicable.

Classification of course in study plans

  • Programme BPCP_CHTPO Bachelor's

    specialization CHPL , 2 year of study, summer semester, compulsory
    specialization PCH , 2 year of study, summer semester, compulsory
    specialization BT , 2 year of study, summer semester, compulsory

  • Programme BKCP_CHTPO Bachelor's

    specialization PCH , 2 year of study, summer semester, compulsory
    specialization BT , 2 year of study, summer semester, compulsory
    specialization CHPL , 2 year of study, summer semester, compulsory

  • Programme BKCP_AAEFCH Bachelor's 2 year of study, summer semester, compulsory
  • Programme BKCP_CHCHTE Bachelor's 2 year of study, summer semester, compulsory
  • Programme BKCP_CHTM Bachelor's 2 year of study, summer semester, compulsory
  • Programme BKCP_CHTOZP Bachelor's 2 year of study, summer semester, compulsory
  • Programme BPCP_AAEFCH Bachelor's 2 year of study, summer semester, compulsory
  • Programme BPCP_CHCHTE Bachelor's 2 year of study, summer semester, compulsory
  • Programme BPCP_CHTM Bachelor's 2 year of study, summer semester, compulsory
  • Programme BPCP_CHTOZP Bachelor's 2 year of study, summer semester, compulsory

  • Programme BPCP_CHTP Bachelor's

    specialization CHPL , 2 year of study, summer semester, compulsory
    specialization PCH , 2 year of study, summer semester, compulsory
    specialization BT , 2 year of study, summer semester, compulsory

  • Programme BKCP_CHTP Bachelor's

    specialization CHPL , 2 year of study, summer semester, compulsory
    specialization PCH , 2 year of study, summer semester, compulsory
    specialization BT , 2 year of study, summer semester, compulsory

  • Programme BPCP_MPMU Bachelor's 2 year of study, summer semester, compulsory

Type of course unit

 

Laboratory exercise

52 hod., compulsory

Teacher / Lecturer

Syllabus

1. Introduction to practice, safety of work, methodology of work in analytical laboratory
2. Precipitation titration (Argentometry)
3. Automatic titration (alkalimetry)
4. Titration in a non-aqueous medium
5. Spectrophotometry
6. Multi-component analysis
7. Fluorimetry
8. Emission flame spectrometry
9. Voltammetry and electrogravimetry
10. Extraction spectrophotometry
11. Liquid Chromatography
12. Thin-layer chromatography