Detail publikačního výsledku
Application of GCxGC-TOF MS for the analysis of drug residues in wastewaters and surface waters
LACINA, P.; VÁVROVÁ, M.; MRAVCOVÁ, L.; ČÁSLAVSKÝ, J.
Originální název
Application of GCxGC-TOF MS for the analysis of drug residues in wastewaters and surface waters
Anglický název
Application of GCxGC-TOF MS for the analysis of drug residues in wastewaters and surface waters
Druh
Abstrakt
Originální abstrakt
This study is focused on the determination of 10 acidic drugs mainly from the group of non-steroidal anti-inflammatory drugs (NSAID) in wastewater and surface water. Target compounds were follows: salicylic acid, acetylsalicylic acid, clofibric acid, ibuprofen, caffeine, naproxen, mefenamic acid, ketoprofen and diclofenac. Samples of wastewater were collected daily in November 2010 from the influent and effluent of the WWTP in Brno – Modřice in Czech Republic. Samples of surface water were collected from significant river stream Svratka in Czech Republic in October 2010. Solid phase extraction (SPE) was used for extraction and preconcentration of analytes. Comprehensive two-dimensional gas chromatography with mass spectrometric detection Time-of-Flight (GCxGC-TOF MS) was used for final analysis of these compounds as an excellent method for trace and ultra trace analysis of organic compounds, due to its high separation efficiency and sensitivity. Only disadvantage is the necessity to derivatize selected compounds with suitable derivatization reagents in this field of analysis.
Anglický abstrakt
This study is focused on the determination of 10 acidic drugs mainly from the group of non-steroidal anti-inflammatory drugs (NSAID) in wastewater and surface water. Target compounds were follows: salicylic acid, acetylsalicylic acid, clofibric acid, ibuprofen, caffeine, naproxen, mefenamic acid, ketoprofen and diclofenac. Samples of wastewater were collected daily in November 2010 from the influent and effluent of the WWTP in Brno – Modřice in Czech Republic. Samples of surface water were collected from significant river stream Svratka in Czech Republic in October 2010. Solid phase extraction (SPE) was used for extraction and preconcentration of analytes. Comprehensive two-dimensional gas chromatography with mass spectrometric detection Time-of-Flight (GCxGC-TOF MS) was used for final analysis of these compounds as an excellent method for trace and ultra trace analysis of organic compounds, due to its high separation efficiency and sensitivity. Only disadvantage is the necessity to derivatize selected compounds with suitable derivatization reagents in this field of analysis.
Klíčová slova
GCxGC-TOF MS, SPE, derivatization, wastewater, surface water
Klíčová slova v angličtině
GCxGC-TOF MS, SPE, derivatization, wastewater, surface water
Autoři
LACINA, P.; VÁVROVÁ, M.; MRAVCOVÁ, L.; ČÁSLAVSKÝ, J.
Rok RIV
2012
Vydáno
07.12.2011
Místo
Clermon-Ferrand
Kniha
12th European Meeting on Environmental Chemistry, Book of Abstracts
BibTex
@misc{BUT75478,
author="Petr {Lacina} and Milada {Vávrová} and Ludmila {Mravcová} and Josef {Čáslavský}",
title="Application of GCxGC-TOF MS for the analysis of drug residues in wastewaters and surface waters",
booktitle="12th European Meeting on Environmental Chemistry, Book of Abstracts",
year="2011",
address="Clermon-Ferrand",
note="Abstract"
}