Detail publikačního výsledku

Fast liquid chromatography as a tool for rapid screening of explosives

ŠESTÁK, J. a kol.

Originální název

Fast liquid chromatography as a tool for rapid screening of explosives

Anglický název

Fast liquid chromatography as a tool for rapid screening of explosives

Druh

Abstrakt

Originální abstrakt

Submitted work assesses a suitability of columns filled with superficially porous particles, Kinetex 2,6 um C-18, Poroshell 120, 2,7 um C-18, and monolithic column Chromolith CapRod RP-18e to perform ultra-fast separation of target explosives. Column permeability and efficiency in wide range of mobile phase velocities were evaluated. Columns filled with superficially porous particles are more efficient than the monolithic one. On the other hand, the monolithic column reaches the best separation impedance. Finally, the superficially porous particles are used when high efficiency and speed are a priority. However, if the pressure drop is limiting factor a monolithic column is a right choice. In this case, the tested monolithic column provided sufficient efficiency for resolution of target explosives in less than 2 minutes.

Anglický abstrakt

Submitted work assesses a suitability of columns filled with superficially porous particles, Kinetex 2,6 um C-18, Poroshell 120, 2,7 um C-18, and monolithic column Chromolith CapRod RP-18e to perform ultra-fast separation of target explosives. Column permeability and efficiency in wide range of mobile phase velocities were evaluated. Columns filled with superficially porous particles are more efficient than the monolithic one. On the other hand, the monolithic column reaches the best separation impedance. Finally, the superficially porous particles are used when high efficiency and speed are a priority. However, if the pressure drop is limiting factor a monolithic column is a right choice. In this case, the tested monolithic column provided sufficient efficiency for resolution of target explosives in less than 2 minutes.

Klíčová slova

fast liquid chromatography, superficially porous particles, monolithic column, explosives

Klíčová slova v angličtině

fast liquid chromatography, superficially porous particles, monolithic column, explosives

Autoři

ŠESTÁK, J. a kol.

Rok RIV

2012

Vydáno

03.11.2011

Nakladatel

librix.eu

Místo

Brno

ISBN

978-80-904959-0-6

Kniha

CECE 2011. 8th International Interdisciplinary Meeting on Bioanalysis

Strany od

65

Strany do

65

Strany počet

1

BibTex

@misc{BUT90682,
  author="Jozef {Šesták}",
  title="Fast liquid chromatography as a tool for rapid screening of explosives",
  booktitle="CECE 2011. 8th International Interdisciplinary Meeting on Bioanalysis",
  year="2011",
  pages="65--65",
  publisher="librix.eu",
  address="Brno",
  isbn="978-80-904959-0-6",
  note="Abstract"
}